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Image Search Results
Journal: Nature Communications
Article Title: Tailored topotactic chemistry unlocks heterostructures of magnetic intercalation compounds
doi: 10.1038/s41467-025-56467-9
Figure Lengend Snippet: a Schematic illustrating four-dimensional scanning transmission electron microscopy (4D-STEM) of a 2 H –TaS 2 flake with a patterned Fe x C y O z precursor. b Mean diffraction patterns, displayed on a logarithmic scale, of 4D-STEM datasets obtained during in-situ heating of a 2 H –TaS 2 flake with a patterned Fe x C y O z precursor. Diffraction reflections of the 2 H –TaS 2 lattice and the Fe superlattice are indicated in violet and red, respectively. The precursor was made by drop-casting a solution of Fe(CO) 5 /isopropanol. Data was collected along the c -axis of the flake after a 30-minute temperature equilibration period. c Plan-view STEM micrograph (∥ c -axis) of a 2 H –TaS 2 crystal with a patterned Fe x C y O z precursor after ex-situ vacuum annealing for 1 hour at 350 °C. The Fe x C y O z precursor was made by drop-casting a solution of Fe(CO) 5 /isopropanol. The 2 H –TaS 2 crystal and the Fe x C y O z patterned precursor are false-colored in blue and red, respectively. Number labels for the TEM grid holes are marked in white. Scale bar: 2 μ m ( d ) STEM-EDS maps of sample ( c ). In the Fe EDS map, 2 H –TaS 2 is outlined in a dashed line. Scale bars: 2 μ m. Selected area electron diffraction (SAED) patterns of ( c ) obtained for grid hole 1 ( e ), hole 2 ( f ), hole 3 ( g ). The Fe/Ta ratio ( x ) is marked on the SAED patterns. First-order diffraction peaks from the 2 H –TaS 2 lattice and the Fe superlattice are highlighted in blue and red, respectively. Scale bars ( e – g ): 5 nm −1 .
Article Snippet: Flakes were transferred onto a 200 nm
Techniques: Transmission Assay, Electron Microscopy, In Situ, Ex Situ